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European Congress of Chemical Engineering - 6
Copenhagen 16-21 September 2007

Abstract 2308 - Methodology for Process Intensification Applied to the Scale-Up of Microreactors

Methodology for Process Intensification Applied to the Scale-Up of Microreactors

Special Symposium - EPIC-1: European Process Intensification Conference - 1

EPIC-1: New Concepts (NC)

MSc Eero Kolehmainen
Lappeenranta University of Technology
Dpt. of Chemical Technology
P.O. Box 20,
FI-53851 Lappeenranta,
Finland
Finland

Dr Ben-Guang Rong
Lappeenranta University of Technology
Department of Chemical Technology
Skinnarilankatu 34,
P.O. Box 20, 53851, Lappeenranta,
Finland
Finland

Prof Ilkka Turunen
Lappeenranta University of Technology
Department of Chemical Technology
P.O.Box 20
FI-53851 Lappeenranta
Finland

Keywords: Process intensification, Microreactor, Scale-up, Creative method, Process phenomena

Methodology for Process Intensification Applied to the Scale-Up of Microreactors

Eero Kolehmainen*, Ben-Guang Rong, Ilkka Turunen

Lappeenranta University of Technology, Department of Chemical Technology, Product and Process Development, P.O Box 20, FIN-53851 Lappeenranta, Finland


Keywords: Process Intensification, Microreactor, Scale-up, Creative method, Process phenomena


Process intensification (PI) is often considered as one of the main current trends in chemical engineering. It has even been suggested as a possible candidate for the third paradigm of the field. The development and applications of process intensification are restricted by the lack of general methodology. Descriptions and suggestions of the methodology have been given e.g. by Green [Chem. & Ind., 1998] and Stankiewicz & Moulijn [CEP, 2000]. However, the essential element of creativity in PI makes the systematic approach very difficult.

Concept such as number-up is regularly used instead of scale-up in the connection of microreactors. This means parallel installation of a large number of microchannels. Design errors may be avoided this way, but other problems appear. Uniform distribution of fluids into many small channels is not easy. Also the investment cost of a microstructured reactor resulting from number-up is inevitably high. Therefore better, innovative scale-up strategies are needed for microreactors.

A new method is suggested for systematic process intensification. It is demonstrated with the scale-up problem of microreactors. The method can be characterized as a combination of phenomena-based reasoning with a creativity technique. Starting from an analysis of relevant physical and chemical phenomena, the goals and partial solutions with their advantages and disadvantages are investigated. This step is called phenomena-based reasoning. The final solution is reached by combining the best partial solutions by removing the restricting contradictions using a creativity technique. As a result, suggestions for favourable construction of microstructured reactors are obtained.



* Corresponding author

Presented Thursday 20, 14:40 to 15:00, in session EPIC-1: New Concepts (NC).

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